MASS SPECTROMETRY ANALYSIS

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INSTRUMENTATION

  • Agilent 6224 Accurate-Mass TOF LC-MS
  • dual electrospray ionization source 
  • multimode electrospray/chemical ionization with atmospheric pressure source
  • mass accuracy = less than 2 ppm, applied m/z range 25 - 20.000 Da
  • acquisition rate 20 spectra/second at m/z 100-3200 (resolution 20.000 FWHM)
  • high performance liquid chromatograph with ultraviolet detection

 

SAMPLES

  • required in solid state (if possible) 1 - 3 mg
  • structure and molecular formula (if known)
  • reagents, impurities and known intermediates description
  • solubility in common solvents (methanol, acetonitrile, chloroform etc.)
  • fotostability, sonication stability, stability in solution, 
  • required analysis - MS or LC/MS

CONTACTS

Mgr. Michal Greguš

(operator, sample reception)

5 4949 6776 (office 307/A14)  gregus(at)mail.muni.cz

Mgr. Eliška Kožuszniková

(operator, sample reception)

5 4949 6776 (office 307/A14) eliska.kozusznikova(at)seznam.cz

Mgr. Vendula Roblová, Ph.D.

(operator, sample reception)

5 4949 6776 (office 307/A14)

roblovavendula(at)gmail.com

Telephone to the lab

5 4949 5939 (laboratory 327/A14)  

Mgr. Miroslava Bittová, Ph.D.

(executive, operator)

5 4949 6454 (office 331/A14)  bittova(at)sci.muni.cz

prof. Mgr. Jan Preisler, Ph.D. 

(guarantee)

  preisler(at)chemi.muni.cz

 

 

  

 

 

 

 

 

 

 

  in Czech crowns/hour

Department of Chemistry Academic institutions

Others

MS analysis

180,- 500,-

1000,-

LC-MS analysis

340,- 1000,- 1500,-